摘要
本文用高效液相色谱法测定了三种赤芍药和脏连丸中芍药甙的含量。用50%乙醇提取样品,超声振荡30分钟;ODS柱分离,甲醇—异丙醇—36%醋酸—水(25:2:2:71)为流动相,检测波长230nm测得四川剥皮赤芍、甘肃赤芍、吉林赤芍、脏连丸中,芍药甙平均含量分别为4.09、2.01、1.94和0.208%。
The paeonifilorin in
three Paeoni lactiflora Pall and Zang li-
an wan was determinated by HPLC.Pae-
oniflorin can be separated on ODS column
with a mobile phase (MeOH: (CH_3)_2CH
OH:36%HAC:H_2O=25:2:2:71) and detected
at 230nm. The samples was treated by
50% MeOH in ultrasonator for 30 min. The
average contents of paeoniflorin are res-
pectively 4.09% (in Sichuan Bopi Paeonia
1.p.) 2.01% (in Gansu Paeonia 1.p.) ,
1.94% (in Jilin Paeonba 1.Pl)and 0.208%
(in Zanglian Wan) .
出处
《华西药学杂志》
CAS
CSCD
北大核心
1990年第3期152-154,共3页
West China Journal of Pharmaceutical Sciences
关键词
赤芍药
芍药甙
脏连丸
含量测定
Daeoniflorin Paeonia lactiflora Pall
Zanglian Wan HPLC
