摘要
本文以蓖麻油为原料,通过醇解,酰胺化得到蓖麻油烷醇酰胺(RA),RA与硼酸进行酯化反应,最终合成了一种新型的有机硼表面活性剂———蓖麻油烷醇酰胺硼酸酯(RAB)。并确定了工艺条件:RA∶H3BO3=2∶1,温度130~140℃。对产物RAB用红外光谱,核磁共振作了表征。
In this paper, methyl ricinolete was prepared by the transesterificationof castor oil with methanol ,followed by acylamination,esterification with H3BO3.The new organoboron surfactant was synthesised.The reaction condition is: RA∶H3BO3=2∶1,reaction temperature 130~140℃.The chmical strusture of Ricioleic alkyl alcohol acylamide borate (RAB) was confirmed by IR,NMR.