N,N′-双(2-叠氮乙基)草酰胺的合成及性能

SYNTHESIS AND PROPERTIES OF N,N BIS (2AZIDOETHYL) OXALIC AMIDE

合成了一种新的化合物Ｎ，Ｎ′双（２叠氮乙基）草酰胺（ＡＥＯ），并鉴定了其结构。通过Ｘ光电子能谱（ＸＰＳ）等仪器对ＡＥＯ与ＨＭＸ的键合作用及ＡＥＯ与硝酸酯和聚醚的相容性进行了研究。结果表明，ＡＥＯ与ＨＭＸ具有键合效果。

A new compound, N,N′bis(2azidoethyl) oxalic amide (AEO), was synthesized and its structure was identified by IR, 1 H NMR,13 C NMR and CIMS elemental analysis. The binding effect of AEO/HMX and the compatibilities of AEO with nitrates and polyethers were studied by XPS and DTA respectively. The results show a application of AEO as a bonding agent for HMXbased PBXs.