合成三氨基三硝基苯的新方法

A NEW METHOD OF SYNTHESIZING 1,3,5TRIAMINO2,4,6TRINITROBENZENE

采用３，５二氯苯胺和三聚氰氯为原料缩合生成Ｎ，Ｎ′，Ｎ″三（３′，５′二氯苯胺基）三聚氰胺（１），缩合产物经硝化、氨化即得三氨基三硝基苯（ＴＡＴＢ），得率８０％。整个过程易于实现。

A new method is discribed for synthesizing 1,3,5triamino2,4,6trinitrobenzene by condensation reaction of 3,5dichloroaniline and tricyanogen chloride, the condensation product is then nitrated and aminated with a yield of 80% compared with the traditional method, this procedure is easy to realize and the cost of starting materials is relatively inexpensive. 