钕—钼杂多配合物(NH_4)_(12)H_(10)[Nd_4Mo_(29)O_(104)(H_2O)_(12)]·22H_2O及Na_4(NH_4)_(10)[Nd_4Mo_(29)O_(100)(H_2O)_(16)]·34H_2O的合成和表征

Study on Synthesis and Chraacterizatiin of Neodrinium Heteroplymolybdate complexes:(NH_4)_(12)H_(10)[Nd_4Mo_(29)O_(104)(H_2O)_(12)]22H_2O and Na_4)NH_4_(10)[Nd_4Mo_(29)O_(106)(H_2O)_(16)]·34H_2O

本文报导了以镧系元素钕为杂原子和钼形成的杂多配合物（NH4）12H10[Nd4Mo29O104（H2O）12]·22H2O及Na4（NH4）10[Nd4Mo29O100（H2O）16]·34H2O的合成方法。通过无素分析、热分析、红外吸收先谱、XPS对所合成的杂多配合物进行了表征。

Neodymium Heteropolymolybdate complexts:(NH_4)_(12)H_(10)[Nd_4Mo_(29)O_(104)(H_2O)_(12)]22H_2O and (NH_4)_(12)H_(10)[Nd_4Mo_(29)O_(104)(H_2O)_(12)]22H_2O and Na_4)NH_4__(10)[Bd_4Mo_(29)O_(106)(H_2O)_(16)]·34H_2Ohave been prepared and characterized by elemental analyses, TG-DTG. IR AND XPS.