高效液相色谱—质谱联用法检测三七总皂苷中Rg_1和Re的含量

The Highly Effective Liquid Chromatography-Mass Spectrum Unites the Usage to Examine in 37 Total Soap Glucoside Rg_1 and the Recontent

目的:建立了高效液相色谱-串联质谱联用方法,用于人参皂苷Rg_1、Re浓度的同时测定,以期为三七及其制剂的质量控制提供一定的依据。方法:建立高效液相色谱-串联质谱联用方法。结果:建立的HPLC/MS/MS方法灵敏高、结果准确、重现性好、操作简便快速。结论:该法准确、灵敏、特异,适用于三七总皂苷及其制剂中人参皂苷Rg_1和Re浓度的同时测定。

Objective： Established the highly effective liquid chromatography - series mass spectrum to unite with the method, used in ginseng soap glucoside Rgt, the Re density at the same time determination, as 37 and the preparation quality control provides certain basis take the time.Methods：Establishes the highly effective liquid chromatography - series mass spectrum to unite with the method.Results：The establishment HPLC /MS/MS method keen high, the result was accurate, the reproduction quality was good, operation simple tast.Conctusiou： This law accurate, was keen, special and suitable in 37 total soap glucoside and the preparation ginseng soap glucoside Rg1 and the Re density at the same time determination.