摘要
采用JSL-500区域熔化真空定向凝固装置,对TbDyFe超磁致伸缩合金定向凝固轴向择优取向、组织和磁致伸缩性能的研究表明:温度梯度GL≈700K/cm基本不变的条件下,当晶体生长速度V1mm/min时,晶体以平面晶方式生长;16mm/min时,以胞状晶方式生长;V=8─12mm/min时,晶体按胞核晶方式生长(胞状晶向树枝晶转变的初始阶段);当V>15mm/min时,晶体按发达的树枝晶方式生长.保持V=12mm/min不变,当GL≈1000K/cm时,晶体又以胞状品方式生长;GL≈400K/cm时,以发达的树枝晶方式生长平面晶和胞状晶生长的样品,其轴向择优取向为<110>取向,磁致伸缩没有压力效应,性能偏低;胞枝晶方式生长的样品轴向择优取向为<112>取向,磁致伸缩性能优越,10MPaN压应力下,平行于外磁场方向的饱和磁致伸缩系数λ最大值达到0.00175;发达树枝晶生长的样品,轴向<112>择优取向程度减弱,磁致伸缩性能下降。
The device of zone melting directional solidification has been used to investigate the preferred orientation, microstructure and magnetostriction of Tb0.3Dy0.7(Fe, M)1.95 (M=Al,Mn, B) metallic compound. When the temperature gradient GL≈700 K/cm, the growth velocity V mm/min, the crystal grows in plannar interface, 1< V 6 mm/min, in cellular morphology; V=8 - 12 mm/min, in primary dendrite; V > 15 mm/min, in developed delldrite. As V=12 mm/min, GL≈1000 and 400 K/cm, the crystal grows in cellular morphology developed dendrite, respectively. Crystals in cellular morphology are <110> preferred orientation and poor magnetostrictive property. Crystals in primary dendrite with <112> preferred orientation, have a good performance, the maximum value of magnetostriction (A) is 0.00175. Crystals in developed dendrite with part <112> orientation have an inferior property than the former.
出处
《金属学报》
SCIE
EI
CAS
CSCD
北大核心
1998年第2期164-170,共7页
Acta Metallurgica Sinica
基金
航空科学基金!97G51058
关键词
定向凝固
磁致伸缩
择优取向
TBDYFE合金
directional solidification
microstructure
magnetostriction
preferred orientation