摘要
以N-乙基二苯胺为母体,通过Vilsmeier反应、碘化、Heck反应和无溶剂Wittig反应合成了新的不等性双枝有机分子(5),其结构经1HNMR,IR,MS和元素分析表征。研究了5在7种溶剂中的紫外可见吸收和荧光发射性质。
A novel inequality two-branch organic molecule （5） was synthesized from N-ethyldiphenyl- amine by Vilsmeier reaction, iodonation, Heck reaction and solvent-free Witting reaction. The structure was characterized by ^1H NMR, IR, MS and elemental analysis. The optical property of 5 in seven different organic solvent was investigated by UV-vis and fluorescence spectrum.
出处
《合成化学》
CAS
CSCD
北大核心
2009年第1期103-105,111,共4页
Chinese Journal of Synthetic Chemistry
关键词
二苯胺
不等性有机分子
合成
光学性质
diphenylamine
inequality organic molecule
synthesis
optical property
