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3,5-二(2-吡嗪基)-4-氨基-1,2,4-三唑的水热合成及晶体结构 被引量:1

Synthesis and crystal structure of 3,5-di(2-pyrazinyl)-4-amino-1,2,4-triazole
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摘要 3,5-di(2-pyrazinyl)-4-amino-1,2,4-triazole(II) was synthesized through hydrothermal reaction,and the crystal structure was determined by X-ray crystallography.Crystalline was assigned into triclinic system with space group P-1,lattice parameters a=0.62527(2) nm,b=0.6807(2) nm,c=1.2792(4) nm,α=85.833(5)o,β=80.517(5)o,γ=72.405(5)°,V=0.5118(3) nm3,and Z=2.Intermolecular hydrogen bonds extend the molecules of compound(II) into a 2D supramolecular layer.CCDC:666956. 3,5-di (2- pyrazinyl)-4-amino-1,2,4-triazole (Ⅱ) was synthesized through hydrothermal reaction, and the crystal structure was determined by X-ray crystallography. Crystalline was assigned into triclinic system with space group P-1, lattice parameters α=0.62527(2) nm,b =0.6807(2) nm,c=1. 2792(4) nm,α= 85. 833(5)°,β =80. 517(5)° ,γ=72.405(5)°, V= 0.5118 (3) nm3, and Z = 2. Intermolecular hydrogen bonds extend the molecules of compound (Ⅱ) into a 2 D supramolecular layer. CCDC :666956.
机构地区 嘉应学院化学系
出处 《化学研究与应用》 CAS CSCD 北大核心 2009年第2期203-206,共4页 Chemical Research and Application
基金 广东省科技厅计划项目(2006B36703005)资助
关键词 3 5-二(2-吡嗪基)-4-氨基-1 2 4-三唑 水热合成 晶体结构 二维层结构 3,5-di ( 2- pyrazinyl) 4-amino-1,2,4-triazole hydrothermal synthesis crystal structure two-dimensional layer.
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