摘要
3,5-di(2-pyrazinyl)-4-amino-1,2,4-triazole(II) was synthesized through hydrothermal reaction,and the crystal structure was determined by X-ray crystallography.Crystalline was assigned into triclinic system with space group P-1,lattice parameters a=0.62527(2) nm,b=0.6807(2) nm,c=1.2792(4) nm,α=85.833(5)o,β=80.517(5)o,γ=72.405(5)°,V=0.5118(3) nm3,and Z=2.Intermolecular hydrogen bonds extend the molecules of compound(II) into a 2D supramolecular layer.CCDC:666956.
3,5-di (2- pyrazinyl)-4-amino-1,2,4-triazole (Ⅱ) was synthesized through hydrothermal reaction, and the crystal structure was determined by X-ray crystallography. Crystalline was assigned into triclinic system with space group P-1, lattice parameters α=0.62527(2) nm,b =0.6807(2) nm,c=1. 2792(4) nm,α= 85. 833(5)°,β =80. 517(5)° ,γ=72.405(5)°, V= 0.5118 (3) nm3, and Z = 2. Intermolecular hydrogen bonds extend the molecules of compound (Ⅱ) into a 2 D supramolecular layer. CCDC :666956.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2009年第2期203-206,共4页
Chemical Research and Application
基金
广东省科技厅计划项目(2006B36703005)资助