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双邻香草醛席夫碱的合成与表征 被引量:2

Synthesis and Characterization of Bis-(o-vanillin)benzoic Imine Schiff Base
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摘要 用邻香草醛,4,4-二氨基二苯醚为原料合成双邻香草醛(二苯醚)苯亚胺Schiff碱,这是一种具有N,N,O,O-四齿配位的新型Schiff碱,通过红外光谱、紫外光谱,核磁、粉末XRD衍射等对其结构进行了表征。结果表明:在无水乙醇中成功合成了双邻香草醛(二苯醚)苯亚胺Schiff碱,且生成的Schiff碱为晶态物质,熔点为170~172℃。 Bis- (O-vanillin) benzoic imine schiff base was synthesized with o-vanillin and 4,4'-diaminodiphenyl ether as raw materials in ethanol,which is a new type of schiff base with N,N,O,O - four teeth coordinate. Through IR, UV, NMR, XRD diffraction and so on, the structures of the schiff base were characterized. The results showed that it is a kind of crystalline material, its melting point is 170 - 172 %.
出处 《当代化工》 CAS 2009年第1期10-12,共3页 Contemporary Chemical Industry
关键词 邻香草醛 SCHIFF碱 表征 O-vanillin Schiffbase Characterization
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  • 1李淑兰,刘德信,周建华,孟凡芹,杨兆荷.邻香兰素L-甲硫氨酸Schiff碱二吡啶合锌(Ⅱ)配合物的合成、晶体结构和热分解动力学[J].化学学报,1995,53(4):343-348. 被引量:10
  • 2康永军,刘德信,李淑兰,李智红,刘亮,杨兆荷.邻香兰素L-缬氨酸Schiff碱吡啶合锌(Ⅱ)配合物的合成、晶体结构和热分解动力学[J].化学学报,1996,54(9):893-899. 被引量:5
  • 3唐波 刘阳 唐晓玲.Chem J Chin Univ(高等学校化学学报)[J],2001,22(6):919-919.
  • 4王建华 杜军.Chin J Appl Chem(应用化学)[J],1999,16(3):114-114.
  • 5高月英 徐克伟 毛岳淦.Acta Chim Sin(化学学报)[J],2001,59(8):1-1.
  • 6刘卫 奚祖威.Chin J Catal(催化学报)[J],1990,11(2):152-152.
  • 7马会宣 胡道道 房喻.Chin J Appl Chem(应用化学)[J],2001,18(4):290-290.
  • 8陈新斌 朱申杰 桂明德.Chem J Chin Univ(高等学校化学学报) [J],2000,21(7):1-1.
  • 9Jin G X, Zhang D. Micron-granula polyethylene with a self-immo- bilized nickelⅡ-α-diimine catalyst bearing two allyl groups. J Polym Sci, Polym Chem, 2004, 42(4): 1018~1024
  • 10Tang G R, Jin G X, Weng L H. Self-immobilized metallocene catalysts bearing an allyl group for ethylene polymerization, X-ray crystal structure of [(CH2=CHCH2)CH3Si(C13H8)2]ZrCl2. J Organomet Chem, 2004, 689(2): 678~684

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  • 1Grabowska A, Kownacki K, Karpiuk J, et al. Photochromism and proton transfer reaction cycle of new internally H-bonded Schiff bases [ J ]. Chemical Physics Letters, 1997,267 : 132 - 140.
  • 2Baser M A,Jadhav V D,Phule R M. Synthesis and antibacterial activity of some new Schiff bases [ J]. Oriental Journal of Chem- istry ,2000,16 (3) :553 - 556.
  • 3Nyarku S K, Mavuso E. Preparation, characterization and biolog- ical evaluation of a chromium ( Ⅲ ) Schiff bases complex derived from o-nitrobenzalhyde hyde and p-paminophenol [J]. South Af- rica Journal of Chem,1998, 51 (4) : 168 - 172.
  • 4Yong L, Huang J. Synthesis of titanium ( Ⅳ) complexes with Schiff bases ligand and their catalytic acticities for polymerization of ethylene and rtyrene [ J ]. Chinese Journal of Chemistry,2001 , 19(4) :429 -432.
  • 5Mirkhani V, Moghadam M, Tangestaninejad S, et al. Catalytic epoxi- dation of olefins with hydrogen peroxide by hybrid complex containing nickel(Ⅲ) Schiff base complex covalently linked to pelyoxometalate [J]. Applied Catalysis A:Genera1l2008,334(1/2) :106 - 111.
  • 6Pelotier B, Anson M S, Campbell I B, et al. Enantioselective sulfide oxidation with H2O2 : a solid phase and array approach for the optimisation of chiral Schiff bases-vanadium catalysts [ J ]. Synlett, 2002, 7: 1055-1060.
  • 7吴兰儿.抗癫痫药新药香荚兰醛通过鉴定[J]药学通报,1982(06):11-13.
  • 8F.Edelkraut. Dissolved vanillin as tracer for estuarinelignin conversion[J].Estuarine Coastal and Shelf Science,1996.737-745.
  • 9Gianni cordano,Jacqueline pezoa,Sergio munoz. Inhibitory effect of vanillin-like compounds on respiration and growth of adenocarcinoma TA 3 and its multiresistant variant TA3-mtx-R[J].European Journal of Pharmaceutical Sciences,2002.255-263.
  • 10仇缀百.药物设计学[M]北京:高等教育出版社,199980-126.

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