交联剂TMPTMA的合成研究

Study on TMPTMA (Cross-Linking Agent) Synthetic Method

对TMPTMA合成的工艺参数进行研究,结果表明,最佳工艺条件:MA/YMP=3.6/1(摩尔比),HQ/TMP=0.19～0.26/1(摩尔比),TSA/TMP=0.2/1(摩尔比),溶剂用量为每摩尔TMP250～400mL,回流反应7～12h。按此工艺条件实验,能获得高收率、高含量的TMPTMA。

By the research of synthetic technology parameter of TMPTMA, the result shows that the best technology conditions are as： MA：YMP =3.6：1（mol ratio）, HQ：TMP = 0.19-0.25：1（mol ratio）, TSA：TMP=0.2：1（mol ratio）,solvent volume 250-400mL/mol TMP,reflux reaction：7-12h. As this technology conditions, TMPTMA can reach to high yield and high content.