摘要
按文献方法合成了不同x值的Et3NHCl-xAlCl3离子液体,并将其用于催化合成苯基二氯化膦,研究了离子液体酸性、用量对反应活性的影响,对其重复使用性进行了考察,并对合成的苯基二氯化膦进行了红外表征。
Et3NHCl-xAlCl3 ionic liquids with different value of x were prepared according to the reference, and the products were used for the catalytic synthesis of dichlorophenylphosphine(DCPP). The effect of acidity and dosages of ionic liquids on the reaction activity was studied, its capacity of reusing was investigated, and the FT- IR was used to analyze the synthesized DCPP.
出处
《化工技术与开发》
CAS
2009年第2期4-5,3,共3页
Technology & Development of Chemical Industry
关键词
离子液体
催化
苯基二氯化膦
ionic liquids
catalysis
dichlorophenylphosphine(DCPP)