摘要
环己基氨基磺酸钠(甜蜜素)的合成最佳工艺实验表明,当氨基磺酸钠、环己胺和轻油的物料比为1:2.5:3.5,反应3h,反应温度165℃时,粗产品经重结晶,产率可达97.5%。轻油和残余的环己胺可通过水蒸气蒸馏回收。
The best technology of sodium cyclamate processing was discussed. The result showed that: amidosulphonic acid, cyclohexylamine and light oil were mixed by the ratio of 1: 2. 5: 3. 5, reacted about three hours under the temperature of 165℃. The crude product was recrystallize, the yield was about 97. 5 percent. Light oil and the residued cyclohexylamine were recovered through the vapour distillation.
出处
《食品科学》
EI
CAS
CSCD
北大核心
1998年第4期15-17,共3页
Food Science
关键词
甜味剂
合成
工艺
甜蜜素
Sweeteners Sodium cyclamate Synthetic technology condition