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Preparation of lead sulfate powder directly from galena concentrates 被引量:1

Preparation of lead sulfate powder directly from galena concentrates
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摘要 A new approach to prepare PbSO4 powder is studied. Using the methods of the leaching of galena concentrates in the ferric chloride media,selective purification and chemical sedimentation,PbS concentrate can be converted into PbSO4. The conversion recovery is 97.39%,the purity of PbSO4 powder is above 99% and its average crystallite size is about 42 nm. In this process,emission of lead vapour and SO2 cannot occur. The experimental results demonstrate the feasibility of realizing a green route to prepare the lead sulfate powder. A new approach to prepare PbSO4 powder is studied. Using the methods of the leaching of galena concentrates in the ferric chloride media, selective purification and chemical sedimentation, PbS concentrate can be converted into PbSO4. The conversion recovery is 97.39%, the purity of PbSO4 powder is above 99% and its average crystallite size is about 42 nm. In this process, emission of lead vapour and SO2 cannot occur. The experimental results demonstrate the feasibility of realizing a green route to prepare the lead sulfate powder.
出处 《中国有色金属学会会刊:英文版》 EI CSCD 2009年第2期479-483,共5页 Transactions of Nonferrous Metals Society of China
基金 Project(50774094) supported by the National Natural Science Foundation of China
关键词 硫化铅精矿 方铅矿 硫酸铅 粉末 PbSO4 制备 平均晶粒尺寸 三氯化铁 lead sulfate galena preparation leaching purification
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