摘要
详细研究了反应温度、反应时间、催化剂用量及物料配比对脂肪醇聚氧乙烯醚羧甲基化反应的影响,优选出最适反应条件。利用薄层色谱、红外光谱对反应产物进行分离提纯和结构分析。图6。
Abstract The title product is prepared by adding 1 mol fatty alcohol polyoxethylene ether into an organic synthetic instrument, then putting 2 mol ground solid sodium hydroxide into it under a strong stirring and slight cooling condition. The experimental temp must be well controlled (namely the temp can't be suddenly raised) 1 mol chloro acetic acid is added into the system, when sodium hydroxide is fully dissolved in it. The reaction is kept for 4 hr. After cooling the product is obtained.
出处
《皮革化工》
1998年第3期17-20,共4页
Leather Chemicals