摘要
本文采用N,N—二甲基甲酰胺作溶剂,以异氰尿酸,苄氯为原料合成了异氰尿酸三苄基酯。通过正交试验探讨了几种因素对产率的影响,在优惠工艺条件下,异氰尿酸三苄基酯的产率达85%以上。
In the paper,tribenzyl isocyanurate was prepared by reaction of isocyanurin acid with benzyl chloride,and in the reaction N,N-dimethyl forma-mide was used as solvent. The effeot of some factors on the yield was discussed by cross cut test. Under the optimum conditions,the yield of tribenzyl isocyanurate was over 85%
基金
湖南省自然科学基金资助项目
关键词
异氰尿酸
异氰尿酸三苄基酯
合成
Isocyanuric acid,Tribenzyl isocyanurate, Synthesis