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One-pot synthesis of(Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propanoic acid 被引量:1

One-pot synthesis of(Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propanoic acid
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摘要 One-pot simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propa- noic acid in DMF (for alkyl amines) or DMF-pyridine (for aryl amines) using a diverse range of alkyl and aryl amines under microwave irradiation condition stereoselectively afforded (Z)-4-(2-bromovinyl)benzenesulfonamides in good yields. One-pot simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propa- noic acid in DMF (for alkyl amines) or DMF-pyridine (for aryl amines) using a diverse range of alkyl and aryl amines under microwave irradiation condition stereoselectively afforded (Z)-4-(2-bromovinyl)benzenesulfonamides in good yields.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第1期48-51,共4页 中国化学快报(英文版)
基金 supported by the Natural Science Foundation of Shanghai,China(No.06ZR14085) by the Scientific Research Foundation for the Returned Overseas Chinese Scholars,State Education Ministry
关键词 ONE-POT Arylsulfonamide (Z)-Arylvinyl bromide Amine Microwave irradiation One-pot Arylsulfonamide (Z)-Arylvinyl bromide Amine Microwave irradiation
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