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A convenient one-step preparation of diaminonitrile compounds

A convenient one-step preparation of diaminonitrile compounds
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摘要 A new method for preparation of diaminonitrile compounds is reported. In this method primary aliphatic diamine compounds were condensed with two equivalents of benzaldehyde and sodium cyanide in presence of an aqueous solution of sodium hydrogensulfite under mild conditions. This method provides an efficient, convenient and practical method for the syntheses of diaminonitrile compounds and the products are easily isolated. The prepared new compounds were characterized by elemental analysis, IR, NMR spectroscopies and mass spectrometry. A new method for preparation of diaminonitrile compounds is reported. In this method primary aliphatic diamine compounds were condensed with two equivalents of benzaldehyde and sodium cyanide in presence of an aqueous solution of sodium hydrogensulfite under mild conditions. This method provides an efficient, convenient and practical method for the syntheses of diaminonitrile compounds and the products are easily isolated. The prepared new compounds were characterized by elemental analysis, IR, NMR spectroscopies and mass spectrometry.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第3期261-264,共4页 中国化学快报(英文版)
基金 the University of Mazandaran of Islamic Republic of Iran for financial support.
关键词 Strecker reaction Diaminonitdle Synthesis CYANIDE One-step preparation Aliphatic diamine Strecker reaction Diaminonitdle Synthesis Cyanide One-step preparation Aliphatic diamine
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