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Synthesis and characterization of A1 doped δ-laminar crystal sodium silicate

Synthesis and characterization of A1 doped δ-laminar crystal sodium silicate
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摘要 An modified laminar crystal sodium silicate (A1-SKS-6) was synthesized by spray drying and high temperature crystallization using sodium silicate as silicon source, A1 atom as inorganic source and hexadecyltrimethy ammonium bromide (CTMAB) as the structure template. The hydrothermal stability of product was at least 1 h. The synthesized material was characterized by XRD and SEM. The results indicated that shape and intensity of XRD diffraction peak at 20 took changes, but raw material 8 phase crystal form kept unchanged, and assured high Ca^2+ and Mg^2+ binding capacity of the products. The Ca^2+ and Mg^2+ binding capacity of product is up to 380 mg Ca/g and 410mg Mg/g respectively. It was found that the hole of product became smaller and appeared rod structure based on SEM. The hydrothermal stability was increased due to the pillaring of AI atom. An modified laminar crystal sodium silicate (A1-SKS-6) was synthesized by spray drying and high temperature crystallization using sodium silicate as silicon source, A1 atom as inorganic source and hexadecyltrimethy ammonium bromide (CTMAB) as the structure template. The hydrothermal stability of product was at least 1 h. The synthesized material was characterized by XRD and SEM. The results indicated that shape and intensity of XRD diffraction peak at 20 took changes, but raw material 8 phase crystal form kept unchanged, and assured high Ca^2+ and Mg^2+ binding capacity of the products. The Ca^2+ and Mg^2+ binding capacity of product is up to 380 mg Ca/g and 410mg Mg/g respectively. It was found that the hole of product became smaller and appeared rod structure based on SEM. The hydrothermal stability was increased due to the pillaring of AI atom.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第4期462-464,共3页 中国化学快报(英文版)
关键词 A1 doping δ-Laminar crystal sodium silicate Detergent builder STABILITY A1 doping δ-Laminar crystal sodium silicate Detergent builder Stability
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参考文献6

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