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胍基化试剂的制备及其应用 被引量:2

Preparation and Application of Guanidinylation Reagents
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摘要 制备了两种胍基化试剂:N-硝基-1-(3,5-二甲基吡唑)脒1,N,N-二叔丁氧羰基硫脲2,将一系列胺类化合物分别与两种胍基化试剂作用,制得新化合物1a-1j,2a-2j,并对两种胍基化试剂的性能进行了比较.所有新化合物的结构均经IR,1HNMR和元素分析证实. Two guanidinylation reagents have been prepared: 3,5-dimethyl-N-nitro-l-pyrazole-l-carboxamidine (DMNPC) land N, N'-bis(tert-butoxycarbonyl)thiourea 2. A series of new compounds 1a-1j, 2a-2j have been synthesized by the reaction of two guanidinylation reagents with amines respectively, and compared character of the two guanidinylation reagents. The structures of all compounds were established by IR, ^1H NMR and elemental analysis.
出处 《新疆大学学报(自然科学版)》 CAS 2009年第2期207-211,共5页 Journal of Xinjiang University(Natural Science Edition)
基金 国家自然科学基金(No.20462006) 新疆植物资源与天然产物化学重点实验室资助项目
关键词 胍基化试剂 制备 应用 guanidinylation reagents lareparation application
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参考文献13

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共引文献13

同被引文献12

  • 1杨浩,吴公信,张振明,高山,冯溶,梁敏,孙克.3-甲基-4-硝基亚胺基全氢化-1,3,5-二嗪的合成[J].农药,2006,45(1):24-25. 被引量:5
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  • 8韩新才,张林,彭华松,方玲,柯文语,贾正涛,吴引超.几种药剂对草坪褐斑病菌的毒力测定[J].武汉工程大学学报,2009,31(7):13-15. 被引量:11
  • 9叶珊珊,王建伟,叶露,邹健锋,单伟光.硫酸胍基丁胺的绿色合成工艺研究[J].浙江化工,2010,41(9):5-7. 被引量:3
  • 10韦鹏,郭睿,孙江,来肖,赵艳艳,孙靖.4-甲基胍基丁酸的合成研究[J].安徽农业科学,2010,38(23):12550-12551. 被引量:2

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