期刊文献+

紫外-可见分光光度法测定噻唑磷含量 被引量:4

Determination of Fosthiazate by UV-VIS Spectrophotometry
下载PDF
导出
摘要 建立紫外-可见分光光度法测定噻唑磷含量的方法。溶剂为正己烷,测定波长为213.9nm,样品质量浓度为36.375mg/L。采用对照比较法计算含量。噻唑磷在23.92~95.68mg/L质量浓度范围内呈线性关系线性相关系数为0.9996。精密度实验RSD不超过0.74%,准确性分析表明噻唑磷的回收率在100.21%~101.16%之间。 A method for determining the content of fosthiazate was established with UV-VIS spectrophotometry, n-hexane as solvent, and the absorptive wavelength was 213.9 nm. The determination of content was 36.375 mg/L. The calibration curve of fosthiazate was linear over the range of 23.92-95.68 mg/L. The linear correlation was 0.9996. The relative standard deviations was not more than 0.74% and the recoveries were from 100.21-101.16%.
出处 《农药》 CAS 北大核心 2009年第5期350-351,共2页 Agrochemicals
基金 山东省博士后创新项目资助专项(200703015)
关键词 紫外-可见分光光度法 噻唑磷 杀虫剂 UV-VIS spectrophotometry fosthiazate pesticide
  • 相关文献

参考文献6

二级参考文献22

  • 1翁建全,刘会君,谭成侠,沈德隆.2-噻唑烷酮的合成研究[J].浙江工业大学学报,2005,33(1):103-105. 被引量:8
  • 2沈德隆,曹炜.噻唑磷的合成[J].农药,2005,44(5):208-209. 被引量:13
  • 3Yasuhiro T,Takao A,Tokya K.Process for the preparation of S,O-dialkyl (2-oxo-3-thiazolidinyl) phosphonothiolates as insecticides,acaricides,nematocides and soil pesticides:JP,63088193[P].1988-04-19.
  • 4Rikuo N,Shinichi K,Nobuyoshi A.Preparation of S,O-dialkyl (2-oxo-3-thiazolidinyl)phosphonothiolates as insecticides,acaricides,nematocides and soil pesticides:JP,02078692[P].1990-03-19.
  • 5Takeshi T,Eiichi R.Asymmetric synthesis of organic phosphorus compounds:JP,2003128688[P].2003-05-08.
  • 6Buck W D,Polotzek-Neudeck J.Process for the preparation of O,Sdialkyl O-aryl thiophosphates:DE,3540989[P].1987-05-21.
  • 7Miller E,Crossley F,Moore M L.Synthesis of Phydroxyphenyl amyl sulfide [J].J Am Chem Soc,1942,64:2323.
  • 8Kawamatsu Yutaka Kogyo K K.Thiazolidine derivatives [P].JP 58177983,1983-10-18.
  • 9Shigeo K,Junichi S.Production of phosphorochloride thiolates [P].US 4290978,1981-09-22.
  • 10Haga T.Organophosphorus based compound,production thereof and insecticide,acaricide,nematicide and agent for killing insect pest in soil containing the same compound [P].JP 2000793,1990-01-05.

共引文献22

同被引文献23

引证文献4

二级引证文献29

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部