摘要
本文采用酸性离子交换树脂作催化剂,己酸和顺-3-己烯醇-1反应得到己酸叶酯,然后对产物进行了红外、质谱、元素分析及多种NMR谱图表征.通过对其1D1HNMR,13CNMR,2DJ分解谱,HMQC等谱图的综合分析,确认了它的结构,并对1H和13C化学位移进行了明确归属.
In this paper, the structure of synthetic cis-3-Hexenyl hexanoate was determined by IR, MS, elemental analysis, NMR spectroscopy. The structural elucidation was supported by the 1D 1H NMR, 13 C NMR, 2D-J-resolved spectroscopy, HMQC of the compound. All the I H and 13C chemical shifts have been assigned on the basis of these experiments.
出处
《中央民族大学学报（自然科学版）》
2009年第2期5-9,15,共6页
Journal of Minzu University of China(Natural Sciences Edition)
