摘要
[目的]建立胆立宁软胶囊质量控制标准。[方法]采用高效液相色谱法,对胶囊中芍药苷进行定量分析,采用薄层色谱法对方中枳壳药材进行定性鉴别。[结果]芍药苷进样量在0.287～5.74μg范围内,进样量与峰面积呈良好线性关系.A=1×106C＋127853,r=0.9995,平均回收率为96.4%,RSD为3.15%;TLC谱检出橙皮苷斑点。[结论]本实验确定的质量控制方法便捷,结果准确可靠、重复性好,可作为胆立宁软胶囊质量控制标准。
[ Objective] To establish quality control method of Danlining soft capsule. [ Methods ] Paeoniflorin content in Danlining soft capsule was determined by HPLC. Semen Arecae were identified by TLC. [ Results ] The linear rage of paeoniflorin was 0. 287 -5.74μg,A = 1 × 10^6C ＋ 127853 ,r =0. 9995. The recorery was 96. 4% , RSD was 3.15% ,The spots of Hesperidin were identified by TLC. [ Conclusion] This quality control wethod was showed rapid reliable and well reproducible.
出处
《实用中医内科杂志》
2009年第5期37-38,共2页
Journal of Practical Traditional Chinese Internal Medicine
关键词
胆立宁软胶囊
芍药苷
橙皮苷
Danlining soft capsule
Paeoniflorin
Hesperidin
