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孕甾-3,6,20-三肟和孕甾-6,20-二酮-3-肟的合成 被引量：7

Synthesis of pregna-3,6,20-trioxime and pregna-6,20-dione-3-oxime
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摘要 Pregna-3,6,20-trioxime and its analog,pregna-6,20-dione-3-oxime were synthesized from pregnenolone by the oxidation of PCC,reduction of NaBH4,oxidation of Jone’s agent and oximation in four-step reaction.Their structures were characterized by NMR and IR. Pregna-3,6,20-trioxime and its analog,pregna-6,20-dione-3-oxime were synthesized from pregnenolone by the oxidation of PCC ,reduction of NaBH4 ,oxidation of Jone＇ s agent and oximation in four-step reaction. Their structures were characterized by NMR and IR.
作者 张晓佳 范磊 李月骅 崔建国
机构地区 广西师范学院化学系
出处 《化学研究与应用》 CAS CSCD 北大核心 2009年第5期726-729,共4页 Chemical Research and Application
基金 国家自然科学基金(批准号:20562001) 广西科学基金(批准号:桂科基0832106) 广西教育厅基金(200707M5172)项目资助
关键词 孕烯醇酮 孕甾-3 6 20-三肟 合成 pregnenolone pregna-3,6,20-trioxime synthesis
分类号 O62 [理学—有机化学]
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化学研究与应用
2009年 第5期

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