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Catalyst-free and solvent-free method for the synthesis of quinoxalines under microwave irradiation

Catalyst-free and solvent-free method for the synthesis of quinoxalines under microwave irradiation
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摘要 A facile procedure for the synthesis, of quinoxalines is being reported starting from benzil and 1,2-diaminobenzene. The reactions were carried out catalyst-free, solvent-free and under microwave irradiation conditions in high yield (84-98%) with short time (3-6 min) and environmental benign, as well as convenient operation. The structures of all the compounds have been confirmed on the basis of their IR, 1H NMR, and/or 13C NMR, mass spectral data. A facile procedure for the synthesis, of quinoxalines is being reported starting from benzil and 1,2-diaminobenzene. The reactions were carried out catalyst-free, solvent-free and under microwave irradiation conditions in high yield (84-98%) with short time (3-6 min) and environmental benign, as well as convenient operation. The structures of all the compounds have been confirmed on the basis of their IR, 1H NMR, and/or 13C NMR, mass spectral data.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第6期672-675,共4页 中国化学快报(英文版)
基金 Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials for financial support(No.JSKC07041)
关键词 QUINOXALINE BENZIL 1 2-Diaminobenzene CATALYST-FREE SOLVENT-FREE Microwave irradiation Quinoxaline Benzil 1,2-Diaminobenzene Catalyst-free Solvent-free Microwave irradiation
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