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Synthesis and characterization ofα-{3-[(2,3-dihydroxy) propoxy]propyl}-ω-butylpolydimethylsiloxanes 被引量:1

Synthesis and characterization ofα-{3-[(2,3-dihydroxy) propoxy]propyl}-ω-butylpolydimethylsiloxanes
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摘要 Hydrosilylation has been carried out between Si-H terminated polydimethylsiloxanes with narrow molecular weight distribution and protected 3-allyloxy-l,2-propanediol, and after subsequently alcoholyzed, α-{3-[(2,3-dihydroxy)propoxy]propyl}-ω- butyl-polydimethylsiloxanes with varying number of ((Si(CH3)2-O) unit were obtained. At each step, the produced compounds were carefully characterized. The results showed that each step was successfully carried out and target products were achieved. Hydrosilylation has been carried out between Si-H terminated polydimethylsiloxanes with narrow molecular weight distribution and protected 3-allyloxy-l,2-propanediol, and after subsequently alcoholyzed, α-{3-[(2,3-dihydroxy)propoxy]propyl}-ω- butyl-polydimethylsiloxanes with varying number of ((Si(CH3)2-O) unit were obtained. At each step, the produced compounds were carefully characterized. The results showed that each step was successfully carried out and target products were achieved.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第6期729-732,共4页 中国化学快报(英文版)
基金 supported by the National Natural Science Foundation of China(No.20576117 and No.20836007)
关键词 POLYDIMETHYLSILOXANE Anionic ring-opening polymerization HYDROSILYLATION ALCOHOLYSIS Polydimethylsiloxane Anionic ring-opening polymerization Hydrosilylation Alcoholysis
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