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嘧啶肟草醚5%乳油的高效液相色谱测定 被引量:6

Determination of Pyribenzoxim 5% EC by HPLC
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摘要 叙述了采用高效液相色谱外标法,以甲醇-水作为流动相,用C18柱和紫外检测器(232nm),测定了嘧啶肟草醚5%乳油的含量。结果表明:方法的标准偏差为0.046;变异系数为0.87%;平均回收率为99.37%;线性相关系数为0.9994。 A quantitative analytical method of Pyribenzoxim 5% EC by HPLC was described in this paper. Using methanol: water -85 : 15(V/V) as mobile phase, using Kromasil C18 column at UV detector (232nm). The results showed that the standard deviation, the coefficient of variation,the average recovery and the liner correlation of method were 0.046,0.87% ,99.37% and 0.9994 respectively.
作者 杨俊柱
出处 《安徽化工》 CAS 2009年第3期69-71,共3页 Anhui Chemical Industry
关键词 嘧啶肟草醚 HPLC 测定 Pyribenzoxim HPLC determination
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  • 1罗亮明,陶贤鉴,黄超群.氰氟草酯的合成[J].农药研究与应用,2007,11(1):23-25. 被引量:8
  • 2Koo Suk Jin, Aim Sei-Chang, Lim Jae Suk, et al. Biological Activity of the New Herbicide LGC-40863 fbenzophenone O-[2,6-bis[(4,6- dimethoxy-2-pyrimidinyl) oxy]benzoyl]oxime} [J]. Pesticide Science, 1997, 51 (2): 109- 114.
  • 3Hur Chang Uk, Cho Jin Ho, Hong Su Myeong, et al. Pyrimidine Derivatives, Process for Their Preparation, and Their Use as Herbicides: EP, 658549 [P]. 1995 - 06 - 21.
  • 4Kim Kun-Tai, Lee Byoung-Bac, Joe Goon-Ho, et al. Process for Preparing 2,6-Di (4,6-dimethoxypyrimidin-2- yl)oxybenzoic Acid Oxime Ester Derivatives as Herbicides: CA, 2194080 [P]. 1997 - 06 - 29.
  • 5Tae-Sook Jeong, Mi Jeong Kim, Hana Yu, et al. (E)-Phenyl- and-heteroaryl-substituted O-benzoyl-(or acyl) oximes as Lipoprotein- associated Phospholipase A2 Inhibitors [J]. Bicorganic & Medicinal Chemistry Letters, 2005; 15: 1524- 1527.
  • 6许昌旭,赵振镐.等.新璎除草剂的嘧啶衍生物、其制备方法及其作除草剂的用途[P].CN:94117926,1995-11-15.
  • 7徐德锋.一种嘧啶水杨酸类除草剂嗡啶肟錾醚的制备方法[P].CN:201310228135,2013-09—25.
  • 8陈晓林,董丰收,刘新刚,郑永权,何林,姚建仁.嘧啶肟草醚在水稻田土壤、植株和大米中的残留分析方法[J].农药,2008,47(5):361-362. 被引量:4
  • 9付启明,欧晓明.巴斯夫除草剂嘧啶肟草醚拟在美国上市[J].农药研究与应用,2009,13(3):52-52. 被引量:3
  • 10邰海军,朱传明.10%氰氟草酯乳油的反相高效液相色谱测定[J].安徽化工,2010,36(2):64-66. 被引量:4

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