摘要
为了分析腰果酚中的有效成分,采用红外光谱仪(IR)对腰果酚进行初步定性;然后采用气相-质谱联用仪(GC/MS)对腰果酚有效成分进行有效分离和准确定性。色谱柱:DB-5柱(30mm×0.25mm×0.25μm);溶剂:氯仿;柱温:起始温度210℃(保持3.0min),升温速率1℃/min,最终温度230℃(保持3.0min)。在此条件下,腰果酚中的有效成分可以较好的分离。
In order to analyze the active composition of cardanol, the preliminary analysis of it was carried out by using infrared spectroscopy （1R）; the active composition of cardanol was separated availably and was analyzed truly by using gas chromatograph-mass spectrometer（GC/MS）. Chromatographic column：DB-5 column（30 min×0.25mm×0.25μm）; solvent：chloroform; column temperature： initial temperature 210℃（keeping 3.0 rain）, the effect of rising emperature rate 1 ℃/min, ： final temperature 230 ℃（keeping 3.0 min）. The active composition ofcardanol were separated completely under this chromatographic conditions.
出处
《广东化工》
CAS
2009年第6期169-171,267,共4页
Guangdong Chemical Industry
