二(1-苯基-3-甲基-4-苯甲酰吡唑啉酮-5)合钯(Ⅱ)的热分解机理

THERMOANALYSIS OF BIS[1-PHENYL-3-METHYL-4-BENZOYL-PYRAZOLONE-5]PALLADIUM(Ⅱ)

报道了二（１－苯基－３－甲基－４－苯甲酰吡唑啉酮－５）合钯（Ⅱ）的合成、红外表征及非等温热分解动力学．采用微分和积分相结合的方法，推断出了可能的热分解机理及热力学方程．

Synthesis,infrared spectra and thermoanalysis of bis (1 phenyl 3 methyl 4 benzoyl pyrazolone 5)palladium(Ⅱ) were reported.Kinetic parameters were obtained from analysis of the TG,DTG curves by integral and differential methods.The possible reaction mechanism was suggested by comparision with the kinetic parameters.