摘要
设计了一种合成标题化合物的新方法,以Z-2-碘-2-丁烯醛为起始原料,通过碘代、还原和酯化合成出了目标产物,总收率81.1%。产品的结构经1HNMR、高分辨质谱确证。
A new method for synthesis of Z-2-iodo-2-butenyl mesylate was reported. It was synthesized through a-iodination, reduction and esterification using Z-2-butenal as the starting materim with an overall yield of 81.1%. The structure of the target product was confirmed by 1HNMR and HRMS.
出处
《化学试剂》
CAS
CSCD
北大核心
2009年第5期387-388,共2页
Chemical Reagents
基金
广西自然科学基金项目(桂科自0899025)
广西高校重点建设实验室-桂西北特色资源研究与开发实验室资助项目(桂教科[2006]4号)
