超声法合成VOPO_4/十六烷基胺插层复合物

Synthesis of intercalated compound VOPO_4/16—Alkylamine by means of ultrasonic method

采用超声合成方法,在短时间内合成了VOPO_4/十六胺插层复合物。对所合成的复合物进行了x—射线粉末衍射、热重分析、元素分析、红外光谱等测定,并对反应产物的结构及反应时间对产物的影响作了初步探讨。

The intercalated compound VOPO4/16-Alkylamine is syntheszed in short time by means of ultrasonic method. The compound has been tested for its XRD, thermo gravimery,element, and IR spectra. A brief discussion has been made to the structure of material from the reaction and the influence of reaction time on the material from the reaction.