摘要
为了获得高纯度的6-姜酚肟,以姜油树脂为原料,通过溶剂萃取、肟化反应和硅胶柱真空层析,获得白色晶体,通过紫外光谱、红外光谱、核磁共振谱、质谱等测定所得白色晶体为6-姜酚肟,并证实了其存在顺反异构。
In order to get pure 6-gingerol oxime ,the crude 6-gingerol was extracted from ginger oleoresin. After oximation reaction and the vacuum column chromatography, the white crystal was obtained. Detected by ultraviolet visible, infrared absorption spectrometry, nuclear magnetic resonance and mass spectrometry, the white crystal was identified as 6-gingerol oxime and it contained cis and transforms.
出处
《天然产物研究与开发》
CAS
CSCD
2009年第3期445-448,共4页
Natural Product Research and Development
基金
广东省教育厅
广东高校科技成果转化重大项目(cgzhd0806)
广州市番禺区引导项目(2008-z-64-1)
