摘要
建立了离子色谱法测定溴素中的游离氯的分析方法，确定了以亚硫酸钠为还原剂还原溴中的游离氯、水浴蒸发除溴的样品预处理方法及操作条件。方法相对标准偏差为0．68％～1．46％，平均加标回收率在97．4％。
The method for the determination of chlorine in bromine by ion chromatography is established . The method for pretreatment of sample is determined and the operating condition is discussed, The method for pretreatment is to remove bromine with water - bath evaporation and reduce free chlorine in bromine with sodium sulfite. The relative standard deviation is between 0.68% and 1.46%, the average recovery is 97.4%.
出处
《盐业与化工》
CAS
2009年第4期34-36,共3页
Jounral of Salt and Chemical Industry
基金
天津科技大学科学研究基金资助项目(20070225)
关键词
游离氯
溴素
离子色谱法
亚硫酸钠
free chlorine
bromine
ion chromatography
sodium sulfite
