摘要
在酸性介质中，左羟丙哌嗪在高锰酸钾一甲醛体系中产生化学发光，而乙二胺四乙酸的存在可显著增强其发光强度，据此建赢了一种简单、快速测定左羟丙哌嗪的化学发光新方法．在实验的优化条件下，化学发光强度与左羟丙哌嗪的浓度在1．0×10^-8～5．0×10^-6g／mL范围内呈现出良好的线性关系．其检测限（3盯）为3．75×10^-9g／mL，对8．0×10^-7g／mL的左羟丙哌嗪溶液进行11次平行测定，相对标准偏差为3．03％．将本法应用于合成样品中左羟内哌嗪的测定，结果满意．
A flow injection chemiluminescence method for levodropropizine determination, which is based on the enhancement effect of the chemiluminescence produced from the acidic potassium permanganate-formaldehyde-ethylene diamine tetra acetic acid system, is described in this paper. Under optimized conditions, the enhanced CL intensity on the levodropropizine concentration is linear in the range 1 ×10^-8 - 5 ×10^-6 g/mL with a detection limit （3σ） of 3.75×10^-9 g/mL. Relative standard deviation （RSD） is 3.03 % （ n = 11 ） for 8×10^-7 g/mL levodropropizine. The proposed method has been successfully applied for levodropropizine determination in synthetic samples with satisfactory results.
出处
《江西师范大学学报（自然科学版）》
CAS
北大核心
2009年第3期279-281,共3页
Journal of Jiangxi Normal University(Natural Science Edition)
关键词
流动注射
化学发光
高锰酸钾
甲醛
乙二胺四乙酸
chemiluminescence
levodropropizine
acidic potassium permanganate
formaldehyde
EDTA
