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不同Ca/P纳米缺钙羟基磷灰石的微波合成和表征 被引量：2

Microwave Synthesis and Characterization of Nano-sized Calcium Deficient Hydroxyapatite with Different Ca/P Ratio
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摘要 通过微波辐射硝酸钙和磷酸的共沉淀物可以快速合成不同Ca/P比的缺钙羟基磷灰石,利用FT-IR、FT-Raman和XRD对产物进行了表征,EDS测定Ca/P比,TEM观察其形貌。结果表明,通过控制反应条件能得到不同Ca/P比的纳米缺钙羟基磷灰石。 Rapid synthesis of calcium deficient hydroxyapatite with different Ca/P ratio was done by precipitation using calcium nitrate and phosphoric acid and subsequently subjecting to microwave irradiation. The synthesized CDHA was characterized by FT-IR, FT-Raman, and XRD. Ca/P ratio was determined by EDS. Transmission electron microscopy analysis showed needle like or stick like morphology of CDHA. In all, nano-sized CDHA with different Ca/P ratio can be synthesized by controlling reaction condtion.
作者 何立志 冯祖德
机构地区 湘潭市环境保护监测站 厦门大学材料科学与工程学院
出处 《广州化工》 CAS 2009年第4期74-76,共3页 GuangZhou Chemical Industry
基金 福建省科技重大专项资助(2005HZ01-3)
关键词 缺钙羟基磷灰 Ca/P比 非化学计量比 calcium deficient hydroxyapatite Ca/P ratio non-stoichiometry
分类号 TQ174.759 [化学工程—陶瓷工业] TP393.08 [自动化与计算机技术—计算机应用技术]
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参考文献16

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共引文献19

同被引文献16

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广州化工
2009年 第4期

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