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柚皮素、橙皮素和桑色素硫酸酯的合成及其HPLC-MS的鉴定 被引量:10

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摘要 目的:合成柚皮素、橙皮素、桑色素硫酸酯。方法:柚皮素、橙皮素、桑色素在冰浴中与浓硫酸反应2 h,用6 mol/LNaOH终止反应。衍生物用高效液相色谱(HPLC)-大气压化学电离(APCI)-质谱(MS)联用鉴定。结果:有柚皮素、橙皮素和桑色素硫酸酯的生成。结论:此方法可以用于柚皮素、橙皮素和桑色素硫酸酯的合成。
出处 《中成药》 CAS CSCD 北大核心 2009年第7期1085-1087,共3页 Chinese Traditional Patent Medicine
基金 广东省重点学科基金资助(9306)
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