摘要
采用酒精-媒晶剂体系制备果糖-1,6-二磷酸钠盐(FDP),并对其最佳结晶工艺条件进行了研究。在此条件下,FDP的结晶收率和产品纯度分别为95%和99.3%。通过元素分析、红外光谱和核磁共振碳谱等对产品结构进行了研究分析。
Octahydro trisodium salt of fructose-1, 6-diphosphate was preparaed with addition agentethanol, The optimal crystal condition was researched. The yield of crystal-lization and purity of the product were 95% and 99. 3% respectively.
出处
《中国生化药物杂志》
CAS
CSCD
1998年第3期124-126,共3页
Chinese Journal of Biochemical Pharmaceutics
关键词
结晶
结构分析
FDP
FDPNa3.8H2O
Octahydro trisodium salt of fructose-1, 6-diphosphate, Crystallization, Characterization