摘要
由醇、酚或胺与中间体芳酰氯经微波光波组合干法合成了一系列新型光敏性偶氮类分子钳,其结构经1HNMR,IR,MS确证。考察了载体、辐射时间、微波功率、催化剂对受体合成的影响。
A series of novel photoresponsive azo-molecular acceptors have been synthesized by solvent free reaction of glycol or hydroxybenzene et al. with intermediate aryl acyl chloride using microwave and light wave. Their structures were characterized by 1H NMR, IR, MS spectra. Effects of carrier, microwave power, irradiation time and catalyzer on preparation of acceptor were investigated.
出处
《安徽农业大学学报》
CAS
CSCD
北大核心
2009年第3期518-520,共3页
Journal of Anhui Agricultural University
基金
九江学院科技项目(06KJ6)
江西省教育厅科技项目(GJJ08440)共同资助
关键词
偶氮受体
微波光波组合
合成
azo receptor
microwave-light wave
synthesis
