摘要
用二甲苯作溶剂，氯乙酸作催化剂，合成了５、１０、１５、２０－四（３－甲氧基－４－乙酰氧基苯基）卟啉，产率达２５．７％。讨论了反应时间对合成的影响。同时，对该卟啉及其锌、钴配合物初步进行了电子光谱、红外光谱等性质研究。
5,10,15,20tetra(3methoxy4acetoxyphenyl) porphyrin was synthesized using xylene as solvent and chloroacetic acid as catalyst, the yield reached 25.7%. The influence of reaction time on synthesis was discussed. The UV and IR properties of the porphyrin and Zn, Co coordination compound were also investigated.
出处
《青岛化工学院学报（自然科学版）》
1998年第2期136-140,共5页
Journal of Qingdao Institute of Chemical Technology(Natural Science Edition)
关键词
合成
卟啉
锌
钴
配合物
四苯基卟啉
取代
synthesis
porphyrin
Zn, Cocoordination compounds
UV
IR
