摘要
采用缓慢蒸发法培养出化合物1-[4-(1,2,4-三唑-5-硫酮)]-3-对甲氧基苯甲酰基硫脲镍配合物晶体,并通过X-射线单晶衍射法测定了晶体结构,它为P2/n空间群的单斜晶体,晶胞参数为a=1.2577(2)nm,b=0.88790(17)nm,c=1.2628(2)nm,V=1.3304(4)nm3,R1=0.0291和wR2=0.0694。
The single crystals of the complex Ni （ C11H11 N5 O2 S2 ）2 was obtained by slow evaporation method at room temperature and its crystal structure was determined with a X-ray diffractometer. It is a monoclinic crystal, its crystallographic parameters are P2/n space group with a = 1.2577（2）nm, b = 0.88790（17）nm, c = 1.2628（2）nm, V = 1.3304（4）nm^3 , RI = 0.0291 and wR2 = 0.0694.
出处
《化学通报》
CAS
CSCD
北大核心
2009年第9期849-852,共4页
Chemistry
基金
国家自然科学基金项目(200803058)
陕西省自然科学基金项目(2007B08)资助
