2,4-二硝基二苯甲酮的优化合成

Optimisation Synthesis of (2,4-Dinitrophenyl)(Phenyl)Methanone

以甲苯为原料,以正交实验优化反应条件,高收率地合成了2,4-二硝基二苯甲酮.产品结构经核磁、红外光谱、质谱和元素分析进行表征.产品纯度经HPLC/MSD测定为98.24%.

Efficient synthesis （2,4-dinitrophenyl）（phenyl）methanone were prepared from toluene. The reaction conditions were optimized by orthogonal experiment. The structure of product was confirmed with NMR, IR spectrum, MS and Elemental analysis, the purity （98.24%） of product was confirmed with HPLC/MSD.