不对称取代的1,3,5-均三嗪衍生物的合成

Preparation of asymmetrically substituted 1,3,5-s-triazine derivatives

以三聚氯氰和苯酚衍生物为原料,在丙酮和水的混合溶液中,两步反应制备了标题化合物,总产率在78%以上。并对产物的结构进行了体积排除色谱和核磁共振谱的表征。

Asymmetrically substituted 1,3,5-s-triazine derivatives were synthesized from cyanuric chloride and phenol derivatives in acetone/H2O by two-step reactions with an overall yield of 〈78%.The structures of the target compound were characterized by SEC,^1HNMR and ^13CNMR.