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Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation

Solvent-free and catalyst-free method for the synthesis of 2,4,5-triarylimidazoles under microwave irradiation
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摘要 A facile procedure for the synthesis of 2,4,5-lriarylimidazoles is being reported starting from benzil, aromatic aldehyde and ammonium acetate. The reactions were carried out with catalyst-free, solvent-free and under microwave irradiation conditions in high yield (80-99%) with short time (3-5 min) and environmental benign, as well as convenient operation. The structures of the compounds have been confirmed on the basis of their IR, 1H NMR, and/or 13C NMR, MS, and elemental analyzer. A facile procedure for the synthesis of 2,4,5-lriarylimidazoles is being reported starting from benzil, aromatic aldehyde and ammonium acetate. The reactions were carried out with catalyst-free, solvent-free and under microwave irradiation conditions in high yield (80-99%) with short time (3-5 min) and environmental benign, as well as convenient operation. The structures of the compounds have been confirmed on the basis of their IR, 1H NMR, and/or 13C NMR, MS, and elemental analyzer.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2009年第10期1198-1200,共3页 中国化学快报(英文版)
基金 the Jiangsu Key Laboratory for Chemistry of Low-Dimensional Materials for financial support(No. JSKC07041)
关键词 Triarylimidazole BENZIL CATALYST-FREE SOLVENT-FREE Microwave irradiation Triarylimidazole Benzil Catalyst-free Solvent-free Microwave irradiation
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