摘要
以正硅酸乙酯(TEOS)和三乙醇胺为原料、氢氧化钾为催化剂、丙酮作溶剂,通过酯交换反应合成了1-乙氧基杂氮硅三环化合物,并初步探讨了反应条件的影响,并用IR对所合成的产物的结构进行了表征。
1 - ethoxy silatrane was synthesized by means of ester exchange reaction in the presence of TEOS and triethanolamine as raw materials, potassium hydroxide as catalyst and acetone as solvent. Meanwhile the influence of reaction condition has been discussed initially. Moreover, the structure of the terminal compound was characterized by IR spectroscopy.
出处
《安阳师范学院学报》
2009年第5期95-97,共3页
Journal of Anyang Normal University
关键词
杂氮硅三环
有机硅
乙氧基
生物活性
合成
Silatrane
Organic silicon
Ethoxy
Biological activity
Synthesis
