摘要
本文对以脂肪醇或脂肪醇醚为原料,以PCl3或POCl3为磷酸化剂合成磷酸三酯或亚磷酸三酯的工艺条件进行了详细探讨,优选出最佳反应条件。本研究产品可作为皮革加脂剂成分使用,亦可作纺织油剂单体使用。表7,图1。
Abstract PCl 3 of POCl 3 is dropped into Wetting Agent JFC at 30~35℃, raised temp to 120℃, kept this temp for 2h; then air is blown into it to remove HCL, and finally H 2O 2 is added, kept temp at 90~100℃ for the purpose of decolourization and neutralized pH to 7 with NaOH to obtain the prodcut.
出处
《皮革化工》
1998年第5期26-29,共4页
Leather Chemicals