摘要
本文采用熔盐法利用自制的合成装置合成了较纯净的1阶、2阶FeCl3-GIC;探讨了合成条件对插入率、阶结构、反应完成程度等的影响。得到了与前人不同的结论,并有良好的实验重复性。
In this paper, purer stage-1,stage-2 FeCl 3-GIC have been synthesized in a device manufactured by ourselves with melting salt method; and it has been studied that the synthesis conditions are effect to the intercalation ratio, stage structure and the degree of full reaction. Some conclusions have achieved that are different from earlier one.
出处
《西南工学院学报》
1998年第3期16-22,共7页
Journal of Southwest China Institute of Technology
关键词
石墨层间化合物
合成工艺
氯化铁
Graphite intercalation compound
Synthesis technology