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采用气相色谱法测定SOP型合成纤维油剂中Span-60的含量 被引量:1

DETERMINATION OF SPAN-60 IN SOP AGENT FOR SYTHETIC FIBER BY GAS CHROMATOGRAPHY
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摘要 将Span-60水解为山梨醇酐和硬脂酸,再将硬脂酸甲酯化,采用气相色谱法测定硬脂酸的量,并根据Span-60的结构式,计算SOP型合成纤维油剂中该物质的含量。测试方法简便易行,测定结果准确、精密度高,令人满意。 Sorbitanmonosteatate was decomposed into sorbitan and stearic acid. The stearic acid was esterif icated by methyl. The methylstearate was detected by gas chromatography. According to the componsition of sorbitanmonostearate, the content of Span - 60 in SOP agent was calculated. The method was simple, with results right, good reproducibility and satisfactory.
出处 《精细石油化工》 CAS CSCD 北大核心 1998年第6期57-59,共3页 Speciality Petrochemicals
关键词 纤维油剂 Span-60 气相色谱法 测定 SOP agent Span-60 decompostion esterification gas chromatography
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