摘要
目的:分析8个不同产地吴茱萸挥发油的化学成分,为其质量评价提供科学依据。方法:采用水蒸气蒸馏法提取吴茱萸挥发油,用GC毛细管柱进行分离,归一化法测定其相对含量,并用GC-MS法鉴定化学成分。结果:8个不同产地吴茱萸挥发油中共有成分有罗勒烯、3,7-二甲基-1,6-辛二烯-3-醇、[1S-(1α,2β,4β)]-1-乙烯基-1-甲基-2,4-二(1-甲基乙烯基)-环己烷、1α,4aα,8aα-1,2,3,4,4a,5,6,8a-八氢-7-甲基-4-亚甲基-1-(1-甲基乙基)-萘、2-亚甲基-6,8,8-三甲基-三环[5.2.2.0(1,6)]十一烷-3-醇、τ-muurolol、α-杜松烯醇和2-十五烷酮。结论:不同产地吴茱萸挥发油化合物组成有一定差异。
Objective： To analyze the chemical components of the essential oil of the evodiae fructus from various habitats and provide scientific basis for its quality control. Methods： The essential oil was extracted by water-steam distillation and separated by GC capillary column chromatography. The relative contents of chemical components were determined by normalization and were identified by GC-MS method. Results： Eight batches of evodiae fructus from various habitats were determined and showed 8 characteristic common compounds, namely ocimene, 3,7 -dimethyl-1,6-octadien-3 -ol, [ 1S-1 α, 2β,4β ） ] -1 -ethenyl-1 -methyl-2,4 -bis （ 1 -methylethenyl ） - cy- clohexane, 1α, 4aα, 8aα-1 , 2,3,4,4a, 5,6,8 a-octahydro-7-methyl-4-methylene-1 -（ 1 -methylethyl ） - naphthalene, 2-methylene-6,8,8-trimethyl-tricyclo [ 5.2.2.0 （ 1 , 6 ） ] undecan-3-ol, τ-muurolol, α-cadinol, and 2-penta- decanone. Conclusion ： There are some differences on the chemical components of the essential oil of the evodiae fructus from various habitats.
出处
《中国现代中药》
CAS
2009年第11期17-20,27,共5页
Modern Chinese Medicine
基金
"十一五"国家科技支撑计划项目(2006BAI06A01-02)
