摘要
利用魏梯希-霍恩(Witting-Horne)反应合成了标题化合物,通过红外、核磁共振和质谱对产物结构及氘代率进行了表征和分析,结果表明产物氘代率为95%,产物结构符合预定结构。
The deuterated p-divinylbenzene had been synthesized from p-xylene by means of the Witting-Home reaction. The structure of deuterated p-divinylbenzene has been confirmed by FTIR, ^1HNMR and mass spectrometry. Test results have shown that the deuterated ratio of the compound was 95 %.
出处
《化学试剂》
CAS
CSCD
北大核心
2009年第12期974-976,984,共4页
Chemical Reagents