期刊文献+

放电等离子烧结热处理合成Ti_3SiC_2粉体 被引量:3

Ti_3SiC_2 Powders Synthesized by SPS Heat Treatment Method
下载PDF
导出
摘要 采用机械合金化合成TiC和Ti3SiC2混合粉体,用放电等离子烧结(SPS)系统对该粉体进行热处理,以合成高纯Ti3SiC2粉体。结果表明,采用SPS无压热处理可以促进机械合金化粉体在较低温度转变成高纯Ti3SiC2粉体材料。随热处理温度(700~1000℃)的升高,产物中Ti3SiC2的含量相应增加,当热处理温度为900~1000℃时,产物中Ti3SiC2纯度可达98wt%。 TiC and Ti3SiC2 mixed powders were synthesized by mechanical alloying. The mechanical alloying powders were heat treated by spark plasma sintering (SPS) for synthesizing high purity of Ti3SiC2 powders. The results show that pressureless SPS can enhance the rate of mechanical alloying powder transforming to high purity of Ti3SiC2 powders at low temperature. With the increase of heat treatment temperature, Ti3SiC2 content of the products increases. At the temperature of 900-1000℃, Ti3SiC2 content of the products reach 98wt%.
作者 张志俊
出处 《热加工工艺》 CSCD 北大核心 2009年第22期86-87,92,共3页 Hot Working Technology
关键词 TI3SIC2 放电等离子烧结 热处理 Ti3SiC2 spark plasma sintering (SPS) heat treatment
  • 相关文献

参考文献10

  • 1Barsoum N W, El-Raghy T. Synthesis and characterization of a temarkable veramic: Ti3SiC2 [J]. J. Am. Ceram. Soc., 1996,79(7): 1953-1956.
  • 2Sun Z M, Zhang Y,Zhou Y C. Sythesis of Ti3SiC2 powders by a solid-liquid reaction process [J]. Scripta Materlia,1999,41(1):61-64.
  • 3Yang S L, Sun Z M, Hashimoto Hitoshi. Synthesis of Ti3SiC2 powder from 1Ti/ (1+x)Si/2TiC powder mixtures[J]. Journal of Alloys and Compounds, 2004,368(1-2): 318-325.
  • 4Yang S L, Sun Z M, Hitoshi Hashimoto,et al. Ti3SiC2 powder synthesis from Ti/Sifric powder mixtures [J]. Journal of Alloys and Compounds ,2003,358(1-2) : 168-172.
  • 5Yang S L,Sun Z M,Hashimoto Hitoshi,et al. Synthesis of single-phase Ti3SiC2 powder [J]. Journal of the European Ceramic Society, 2003,23(16): 3147-3152.
  • 6Li H, Chen D,Zhou J,et al. Synthesis of Ti3SiC2 by pressureless sintering of the elemental powders in vacuum [J]. Mater. Lett., 2004,58 : 1741-1744.
  • 7金松哲,王蕾,吴化,孙世成,任露泉,杨晨.热处理温度对机械合金化合成Ti3AlC2粉体纯度的影响[J].材料热处理学报,2008,29(3):35-38. 被引量:6
  • 8Zhang Z F, Sun Z M, Hashimoto H. Rapid synthesis of ternary carbide TisSiC2 through pulse discharge sintering technique from Ti/Si/C powders [J]. Metal. Mater. Trans., 2002,33 : 3321-3328.
  • 9Li H,Peng L M,Gong M,et al. Effect of Al on synthesis of Ti3SiC2 by vacuum sintering [J]. Z. Phs. Chem.,2005,219: 1411-1420.
  • 10Sun Z M,Zou Y,Shuji Tada,et al. Effect of Al addition on pressureless reactive sintering of Ti3SiC2 [J]. Scripta Materialia, 2006,55(11): 1011-1014.

二级参考文献10

  • 1Barsoum M W. The MN +1 AXIN phases : a new class of solids : Thermodynamically Stable Nanolaminates[ J]. Prong Solid St Chem, 2000,28 : 201 - 281.
  • 2Tzenov N V, Barsoum M W. Synthesis and characterization of Ti3 AlC2 [ J]. J Am C eram Soc, 2000,83(4):825- 832.
  • 3Myhra S, Crossley J A A, Barsoum M W. Crystal-chemistry of the Ti3 AlC2 and Ti4 AlN3 layered carbide/nitride phases characterization by XPS[ J]. Journal of Phase and Chemistry of Solid,2001,62:811 -817.
  • 4ZHANC Y, SUN Z M, ZHOU Y C. Cu/Ti3SiC2 composite: a new eleetrofriction material[J]. Mater Res lnnovat, 1999, (3):80.
  • 5WANG X H, ZHOU Y C. Mierostrueture and properties of Ti3 AlC2 prepared by the solid-liquid reaction synthesis and simultaneous insitu hot pressing process [J]. Acta Marerialia,2000,50:3141 - 3149.
  • 6LI S B, ZHA1 H X, BE1 G P, et al. Formation of Ti3AlC2 by mechanically inducedself-propagating reaction in Ti-Al-C system at room temperature[J]. Materials Science and Technology, 2006, 22 (6) :667 - 772.
  • 7LI Shi-bo, ZHAI Hong-xiang, BEI Guo-ping, et al. Synthesis and microstructure of Ti3AlC2 by mechanically activated sintering of elemental powders[J]. Ceramics International, 2007,33 : 169 - 173.
  • 8LI Jing-feng, Toshiro Matsukl, Ryuzo Watanabe. Mechanical-alloying-assisted synthesis of Ti3 SiC2 powder[ J]. Journal of the American Ceramic Society, 2002, (4) : 1004 - 1006.
  • 9PENG Chun-qing, WANG Chang-an, SONG Yang, et al. A novel simple method to stably synthesize Ti3 AlC2 powder with high purity[J]. Materials Science and Engineering,2006,428( 1 - 2) :54 - 58.
  • 10Pietzka M A, Schuster J C. Summary of constitutional data on the Al-C-Ti system[J]. Phase Equilib, 1994,15(4) :392.

共引文献5

同被引文献28

  • 1尚书勇,梅丽,李兰英,印永祥,戴晓雁.等离子体法制备超细粉体氮化铝的研究[J].化工新型材料,2004,32(7):8-10. 被引量:5
  • 2蒋显亮,M.BOULOS.Induction plasma spheroidization of tungsten and molybdenum powders[J].中国有色金属学会会刊:英文版,2006,16(1):13-17. 被引量:34
  • 3Fang Z Z, Wang Xu, Ryu Taegong, et al. Synthesis, sintering, and mechanical properties of nanocrystalline cemented tungsten carbide-A review [J]. Iuternational Journal of Refractory Metals and Hard Materials, 2009,27(2): 288-299.
  • 4Fan Jinglian, Liu Tao, Cheng Huichao, et al. Prepartion of fine grain tungsten heavy alloy with high properties by mechanical alloying and yttrium oxide addition [J]. J. Mater. Process Technol., 2008,208(1) :463-469.
  • 5Moriysohi Y, Futaki M, Komatsu S, et al. The preparation and characterization of ultrafine tungsten powder [J]. J. Mater Sci. Let., 1997,16(5): 347-349.
  • 6Hedger H J, Hall A R. Preliminary observations on the use of the induction-coupled plasma torch for the preparation of spherical powder [J]. Powder Me., 1961,8(1) : 65-70.
  • 7高敏,张景韶和Rowe D M.温差电转换及其应用[J].北京:兵器工业出版社.1996.
  • 8Rowe D M. CRC jandbook of thermoelectrics [J]. CRC, Boca Raton, FL, 1995.
  • 9Tani T, Itahara H, Xia C, et al. Topotactic synthesis of highly-textured thermoelectric cobaltites [J]. J. Mater. Chem., 2003,13(8): 1865-1867.
  • 10Ito M, Seo W S, Koumoto K. Thermoelectric properties of PbTe thin films prepared by gas evaporation method [J]. J. Mater. Res,, 1999,14: 209.

引证文献3

二级引证文献6

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部